.
Umwenda ushonga ufite ibiranga ubunini buto bwa pore, uburozi bwinshi no kugikora neza, kandi ni ibintu byingenzi bya mask umusaruro. Iki gikoresho cyerekeza kuri GB / T 30923-2014 Polypropylene (pp) guswera ibikoresho bidasanzwe, bikwiranye na polypropylene nkibikoresho byibanze bya peroxide, hamwe na di-Buy-Butyl ibintu bidasanzwe.
Icyitegererezo kirashonga cyangwa cyabyimbye muri Toluene Solven irimo umubare uzwi wa N-hexane nkimbere. Umubare ukwiye wigisubizo cyashizwemo na microsampler kandi watewe muri gaze thromatograph. Mubihe bimwe, gusesengura gazi chromatografiya byakozwe. Ibisigisigi bya DTBP byagenwe nuburyo busanzwe.
1) Gazi chromatograph, capillary inkingi inlet, statector ya fid,
2) Gusesengura uburinganire
3) Inkingi ya Capillary: kuri.624 30m * 0.32mm * 1.8μm,
4) Porogaramu ikorera Chromatografi,
5) n-hexane, yera ya chromatografi;
6) di-tert-Buyl peroxide, musesenguwe;
7) Toluene, Isuku Yera.
GC-7890 Gaze ya Chromatograph ikubiyemo sisitemu yo kugenzura microcomputer hamwe na ecran nini yo kwerekana, isura ni nziza kandi yoroshye. Urufunguzo rushya rwateguwe rworoshye kandi rwihuta, kandi imizunguruko itumizwa mu mahanga ibice, bityo imikorere yibikoresho irahamye kandi yizewe kandi yizewe.
Ⅰ. Kwishyira hamwe umuriro, gusobanuka cyane, imikorere myinshi
1. Igikorwa Cyingenzi-Microcomputer, 5.7 Inch (320 * 240) Kugaragaza LCD nini .
2.MmicroComputer Kurwanya Hydrogen Statector kugirango igere kumikorere yo gutwika, abanyabwenge benshi. Integrateonal ihuriweho na Digital Strotronic Yumuzunguruko, igenzura ryinshi rusange, imikorere ihamye kandi yizewe, kugeza kuri 0.01 ℃ Porogaramu yubushyuhe.
3.Gas Imikorere yo Kurinda 3.Gas, Kurinda inkingi na pisine yo mu bushyuhe, electron gufata detector.
Ifite imikorere yo kwisuzumisha mugitangira, ifasha abakoresha kumenya vuba impamvu numwanya wo kunanirwa (gupima byoroshye), kunanirwa kw'amashanyarazi), imikorere yo kurwanya imbaraga, Itumanaho rya Data-Power Igikorwa cyo kugenzura kure. Imikorere yo kurinda ubushyuhe irangwa
Igikoresho ntabwo cyangiritse kandi gifite uburyo bwo kwibuka amakuru bidasaba gusubirwamo.
Ⅱ.Sisitemu yo gutera inshinge igishushanyo cyihariye, gishobora kuba ntarengwa
1. Igishushanyo mbonera cyihariye cyo gukemura ivangura; Imikorere ibiri y'indishyi ntabwo ikemura gusa umurongo ukurikiranwa haterwa n'ubushyuhe bwateguwe, ariko nanone ikuramo ingaruka z'urusaku rw'inyuma kugirango ubone imipaka yo gutahura.
2.Inkingi ipakiye, capillary smant / sisitemu yo gutera inshinge (hamwe nimikorere ya diaphragm)
3.Ikora ya gaze yikora / intoki muburyo butandatu, infashanyo yimyanya, injiji yubushyuhe, metani ihinduranya, injiji yikora.
Ⅲ, ubushyuhe bwateguwe, itanura ryasobanutse neza, gushikama byihuse
1.Icyemezo-cyerekana ubushyuhe bwa gahunda, nyuma yumuryango ukoresheje ifoto ihindura igishushanyo mbonera, ubwenge kandi burambye nyuma yumubare wa sisitemu yo kuzamuka Igikorwa cya hafi cyurubuga, ubushyuhe bugenzura neza ± 0.01 ℃, byujuje ibisabwa nisesengura.
2.Gukoresha ingano yinkingi, sisitemu yubwenge inyuma yumuryango uhindagurika umwuka uhumeka ikirere muri no hanze, gabanya gahunda nyuma yo guterura sisitemu ihamye igihe; Gushyushya Itanura: Ubushyuhe bwibidukikije + 5 ℃ ~ 420 ℃.
3.Ingaruka zo kwikinisha ni nziza: Agasanduku k'inkingi, imyuka, gutahura ni dogere 300, agasanduku k'inyuma n'igifuniko cyo hejuru kiri munsi ya dogere 40, kunoza igipimo cy'abakoresha.
4.Usindagura igishushanyo mbonera cy'icyumba cyuzuye, ingano ntoya yapfuye; Ibikoresho byo gusimbuza: Gutera inshinge, liner, umuhuza, ukusanya, nozzle irashobora gusimburwa ukuboko kumwe; Umusimbura mukuru wumubiri: Kuzuza inkingi, icyitegererezo cya capillary na detector birashobora gukurwaho burundu hamwe numutwe gusa, kubungabunga byoroshye.
Ubushishozi buhanitse, gahunda yo gutura cyane, yujuje ibyifuzo bya gahunda zitandukanye
Hydrogen Flame Ionation Detector (FID), Gutezimbere Ubushyuhe Bwimuka (TCD), Electron Gufata Detector (ECD),
Flame Photometric Statector (FPD), Nitroduse na PhoSPhorus detesctor (NPD)
Ubwoko bwose bwa peteroli bushobora kugenzurwa ubushyuhe, hydrogen strimector biroroshye gusenya no gushiraho, byoroshye gusukura cyangwa gusimbuza nozzle.
Icyambu cya inshinge
Ibyambu bitandukanye byatewe inshinge biboneka: Gushinge inkingi yuzuye, shunt / inshinge idashinyagurira capillary
Inkingi yubushyuhe
Ubushyuhe Bwenge: Ubushyuhe bwicyumba + 5 ~ 420 ℃
Igenamiterere ry'ubushyuhe: Impamyabumenyi 1; Ubushyuhe bwateguwe igipimo cyo kuzamuka 0.1
Igipimo ntarengwa cyo gushyushya: dogere 40 / min
Ubushyuhe buhamye: 0.01 Impamyabumenyi Yubushyuhe Yangiza Impamyabumenyi 1
Ubushyuhe bwateguwe: Ubushyuhe bwa 8 Gahunda ya gahunda irashobora guhinduka
Hydrogen flame oonation detector (fid)
Ubushyuhe bukora: 400 ℃
Imipaka ntarengwa: ≤5 × 10-12G / S (n-hexadecane)
Drift: 5 x 10-13 A / 30 min cyangwa munsi yayo
Urusaku: 2 x cyangwa munsi ya 10 kugeza 13 a
Umurongo wa Dynamic Range: ≥107
Ingano: 465 * 460 * 550mm, uburemere: 40kg,
Imbaraga zinjiza: AC220V 50HZ IGIHE CYANE 2500W
Inganda za Shimili, Ibitaro, Petroleum, Ubuseri, Ubugenzuzi bwibidukikije, ubutaka, amashanyarazi, ubucukuzi bw'amashanyarazi, nibindi
Imbonerahamwe ya Ethylene Oxide Iboneza Ibikoresho byubuvuzi:
| Umubare | Izina | Ibisobanuro | umubare wa |
| 1 | Gazi chromatograph | GC-7890 Uwakiriye (SPL + FID) | 1 |
| 2 | Generator yo mu kirere | 2L | 1 |
| 3 | Amashusho ya Hydrogen | 300ml | 1 |
| 4 | Nitrogen | Isuku: 99.999% silinderi + umuvuduko ugabanya valve (yaguzwe mu karere) | 1 |
| 5 | Inkingi yihariye | Capillary Inkingi | 1 |
| 6 | AKAZI | N2000 | 1 |
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